Synthesis of High Purity- Sicand- Si 3N4Fromricehulls

Autores/as

  • B. Treviño Universidad Autónoma de Nuevo León
  • I. Gómez Universidad Autónoma de Nuevo León
  • R. Colás Universidad Autónoma de Nuevo León

DOI:

https://doi.org/10.29105/qh1.3-131

Palabras clave:

Rice hulls, silicon carbide, silicon nitride,, synthesis

Resumen

Silicon carbide and silicon nitride were synthesized from ashes obtained by heating rice hulls at 800C for 3 hours in argon. -SiC
was produced from the ashes by reheating them at l 400C for 8 hours in argon, whereas -Si,N, was obtained by heating the ashes at
temperatures ranging from 1250C to l 400C for periods of 3 to 6 hours in a nitrogen rich atmosphere. Toe products were characterized by infrared spectroscopy, X-ray and scanning electron microscopy. High purity -SiC and -Si,N, compounds with whisker type morphology were obtained. It was possible to obtain -Si,N, without SiC by heating the ashes for 6 hours at 1250C.

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Biografía del autor/a

B. Treviño, Universidad Autónoma de Nuevo León

Centro de Laboratorios Especializados, Facultad de Ciencias Químicas,

I. Gómez, Universidad Autónoma de Nuevo León

Centro de Laboratorios Especializados, Facultad de Ciencias Químicas,

R. Colás, Universidad Autónoma de Nuevo León

Facultad de Ingeniería Mecánica y Eléctrica 

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Publicado

2011-06-30

Cómo citar

Treviño, B., Gómez, I. ., & Colás, R. (2011). Synthesis of High Purity- Sicand- Si 3N4Fromricehulls . Quimica Hoy, 1(3), 32–38. https://doi.org/10.29105/qh1.3-131

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